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Polyketones are generally prepared in a conventional manner by contacting a monomer mixture containing a catalyst compound with molecular oxygen in an oxygen-containing organic solvent, such as an aliphatic hydrocarbon which contains dissolved oxygen. The exact mechanisms by which polyketones are prepared and some of their inherent characteristics are now briefly reviewed. Briefly, a catalyst compound is contacted with an organic solvent which contains dissolved oxygen. The catalyst compound is a transition metal compound comprising a compound of a metal of Groups IB, IIB or VIIIB of the Periodic Table of Elements together with an anion of a non-aromatic hydrocarbon radical ligand which in its free valency state contains at least one reactive hydrogen atom. In some cases the catalyst compound also contains a compound of a non-aromatic hydrocarbon radical ligand of at least one oxygen or sulfur atom of valency at least two. The reaction is generally carried out at a temperature of about 100.degree. to 150.degree. C. under an atmosphere of oxygen, water and hydrocarbon. The presence of catalyst compound as well as
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